Highlightsfrom projekts performed with or in the PSI Hotlab:

Scientific Highlights

Datum
12 April 2022
First combined Plasma and Gas Source Mass Spectrometer for alternate isotope and element ratio Analyses of Solids, Liquids, and Gases

MC-EBIS-ICP-MS – a unique dual Ion Source Mass Spectrometer

This highlight presents a successful, in-house developed integration of an Electron Beam Ion Source (EBIS) able to ionize gases to high charge states with a customized commercial MC-ICP-MS. The successful joining of the two ion flight paths is a milestone towards comprehensive routine analyses of solids, liquids, and gases using THE SAME MASS SPECTROMETER, the latter analyses free from atmospheric contamination. After implementation of an introduction system for gas mass spectrometry, routine analyses will comprise isotope ratio and relative abundance determinations of fission gases in used nuclear fuel. In addition to the unique versatility of the MC-EBIS-ICP-MS, inclusion of the EBIS furthers opens the little-studied field of mass spectrometry of highly charged ions.

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11 March 2019
teaser picture

Cladding tubes and their properties

Energy and Environment Nuclear Power Plant Safety Research Using Neutrons

In the Nuclear Energy and Safety Research Division at PSI, Johannes Bertsch focuses on the so-called cladding tubes that are used in nuclear power plants.

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5 January 2018
Pellet Periphery Teaser

UO2 fuel behavior at very high burnup

The investigation of the nuclear fuel at very high burnup is critical for evaluating the safety margin for the evaluated fuel in normal as well as in accidental conditions. PSI is one of the very few hot laboratories which possess access to irradiated UO2 fuel with very high burnup from commercial reactors. The application of relevant tools for the investigation, handling and analysis of those highly irradiated materials emphasize the necessary expertise.

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5 January 2018
Focused Ion Beam

New Focused Ion Beam (FIB) in the Hot Laboratory

The implementation of Focused Ion Beam instruments in material research laboratories during the last decade has not only strongly improved the preparation of very thin specimens for the Transmission Electron Microscope (TEM), in particular at interfaces, but also led to the development of new analysis methods inside the instrument itself. It became a powerful instrument for the analyses of highly radioactive materials, because it allows for the production and analysis of very small specimens that can be then analyzed with very sensitive detectors without strong interference from the radiation field of the specimen itself.

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3 October 2017

Pt nanoparticles: The key to improved stress corrosion cracking mitigation in boiling water reactors

The formation and growth of cracks by stress corrosion cracking (SCC)in reactor internals and recirculation pipes due to the highly oxidising environment is a serious issue in boiling water reactors. At first, SCC mitigation was attempted by injecting H2 into the feed water, where the injected H2 recombines with the H2O2 and O2 to water and reduces the electrochemical corrosion potential, and consequently the SCC susceptibility. Several disadvantages of the injection of high amounts of H2, have led to the development of noble metal additions to the reactor feed water. With injection of a much smaller amount of H2, the noble metal particles of a few nanometres in size, formed in-situ, work as catalysts for the efficient reduction of the oxidizing species formed by radiolysis, and thus lower the ECP and SCC susceptibility.

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