Publications

Özsoy A, Hearn WA, Gaudez S, Jeswani R, Chen Y, Rack A, et al.
Deconvoluting cracking mechanisms in fusion processing of steel-copper multi-materials via Operando X-ray characterisation
Virtual and Physical Prototyping. 2025; 20(1): e2526798 (27 pp.). https://doi.org/10.1080/17452759.2025.2526798
DORA PSI

Su J, Chen L, Van Petegem S, Jiang F, Li Q, Luan J, et al.
Additive manufacturing metallurgy guided machine learning design of versatile alloys
Materials Today. 2025. https://doi.org/10.1016/j.mattod.2025.06.031
DORA PSI

Ziegelwanger T, Reisinger M, Petersmann M, Van Petegem S, Rodriguez-Lamas R, Todt J, et al.
Intragranular strain and mosaicity in Cu thin films during fast thermomechanical fatigue
npj Materials Degradation. 2025; 9: 79 (13 pp.). https://doi.org/10.1038/s41529-025-00629-z
DORA PSI

Jamili AM, Basu I, Cayron C, Van Petegem S, Jhabvala J, Grundy AN, et al.
Formation mechanism and microstructural characteristics of a body-centered cubic phase in 3D printed 316L–CuCrZr multi-material structures, combining laser powder bed fusion with foils
Scripta Materialia. 2025; 268: 116844 (7 pp.). https://doi.org/10.1016/j.scriptamat.2025.116844
DORA PSI

Olsson M, Klein A, Mozhzhukhina N, Xiong S, Appel C, Carlsen M, et al.
Resolving the sodiation process in hard carbon anodes with nanostructure specific X-ray imaging
Advanced Science. 2025. https://doi.org/10.1002/advs.202508635
DORA PSI

Chen Y, Baroni A, Tänzer T, Nielsen L, Liebi M
Reconstructing three-dimensional optical anisotropy with tomographic Müller-polarimetric microscopy
Advanced Science. 2025: 2502075 (9 pp.). https://doi.org/10.1002/advs.202502075
DORA PSI

Mani D, Cloetens P, Karpov D, Monaco F, Chehab B, Shahani R, et al.
Nanoscale 3D characterization of an Al-1Fe-1Zr alloy for additive manufacturing
Materials Characterization. 2025; 225: 115109 (9 pp.). https://doi.org/10.1016/j.matchar.2025.115109
DORA PSI

Abdesselam KA, Gaudez S, Van Petegem S, Honkimäki V, Hallais S, Cornet L, et al.
Altering microstructure and enhancing mechanical properties during direct energy deposition of Ti-6Al-4V via in-process laser heat treatments
Materials and Design. 2025; 254: 113997 (17 pp.). https://doi.org/10.1016/j.matdes.2025.113997
DORA PSI

Martin N, Denoréaz T, Bambach M, Van Petegem S, Makowska M
Investigation by operando synchrotron X-ray diffraction of the phase transformation in 316L-IN625 multi-material Direct Energy Deposition
Journal of Materials Research and Technology. 2025; 36: 6821-6833. https://doi.org/10.1016/j.jmrt.2025.04.278
DORA PSI

Carlsen M, Malamud F, Modregger P, Wildeis A, Hartmann M, Brandt R, et al.
Texture tomography with high angular resolution utilizing sparsity
Journal of Applied Crystallography. 2025; 58(2): 484-494. https://doi.org/10.1107/S1600576725001426
DORA PSI

Malamud F, Gaudez S, Capek J, Fogliatto EO, Strobl M
Texture analysis implementation at the neutron strain diffractometer POLDI
Materials Characterization. 2025; 224: 115003 (11 pp.). https://doi.org/10.1016/j.matchar.2025.115003
DORA PSI

Muther A, Makowska MG, Zhang ZL, Verga F, Marone F, Garrivier N, et al.
Identifying melt pool behavior in ceramics PBF-LB via operando synchrotron tomographic microscopy and high-fidelity process modeling
Additive Manufacturing. 2025; 103: 104756 (19 pp.). https://doi.org/10.1016/j.addma.2025.104756
DORA PSI

Silva Barreto I, Liebi M, Le Cann S, Ahmed S, Nielsen LC, Grünewald TA, et al.
Lack of embryonic skeletal muscle in mice leads to abnormal mineral deposition and growth
Journal of Structural Biology. 2025; 217(1): 108178 (12 pp.). https://doi.org/10.1016/j.jsb.2025.108178
DORA PSI

Gaudez S, Weisz-Patrault D, Abdesselam KA, Gharbi H, Honkimäki V, Van Petegem S, et al.
Estimating elastic and thermal contributions to lattice strains from operando X-ray diffraction measurements using fast simulations
Additive Manufacturing. 2025; 101: 104674 (15 pp.). https://doi.org/10.1016/j.addma.2025.104674
DORA PSI

Görl D, Haraguchi S, Hryshunin Y, Thiele S, Scetta G, Simula A, et al.
Supramolecular modification of sustainable high-molar-mass polymers for improved processing and performance
Nature Communications. 2025; 16(1): 217 (13 pp.). https://doi.org/10.1038/s41467-024-55166-1
DORA PSI

Rodriguez-Fernandez I, Bretschneider T, Menzel A, Suljevic O, Sommer NG, Weinberg AM, et al.
Physical exercise impacts bone remodeling around bio-resorbable magnesium implants
Acta Biomaterialia. 2025; 193: 623-631. https://doi.org/10.1016/j.actbio.2024.12.008
DORA PSI

Ziegelwanger T, Reisinger M, Vedad B, Hlushko K, Van Petegem S, Todt J, et al.
20 kHz X-ray diffraction on Cu thin films explores thermomechanical fatigue at high strain-rates
Materials and Design. 2025; 251: 113664 (pp.). https://doi.org/10.1016/j.matdes.2025.113664
DORA PSI

Gaudez S, Malamud F, Hearn W, Sumarli S, Strobl M, Van Petegem S
Evolution of texture and residual stresses in 2205 duplex stainless steel during laser powder bed fusion
Materials and Design. 2025; 251: 113658 (13 pp.). https://doi.org/10.1016/j.matdes.2025.113658
DORA PSI

Sumarli S, Polatidis E, Malamud F, Van Petegem S, Busi M, Logé RE, et al.
A downsized laser powder bed fusion device for operando neutron studies: design and experiments
Additive Manufacturing. 2025; 98: 104654 (10 pp.). https://doi.org/10.1016/j.addma.2025.104654
DORA PSI

Ghanbari R, Terry A, Wojno S, Bek M, Sekar K, Sonker AK, et al.
Propagation of orientation across lengthscales in sheared self-assembling hierarchical suspensions via Rheo-PLI-SAXS
Advanced Science. 2025; 12(7): 2410920 (13 pp.). https://doi.org/10.1002/advs.202410920
DORA PSI

Zhang H, Venero DA, Park J, Petegem SV, Özsoy A, Soundarapandiyan G, et al.
Microstructure evolution and precipitation strengthening behaviour of additively manufactured high-speed steels
In: Alphonso WE, Defer MC, Godfrey A, Juul Jensen D, Mohanty S, Nadimpalli VK, et al., eds. 44th Risø international symposium on materials science (RISO 2024). Vol. 1310. IOP conference series: materials science and engineering. IOP Publishing; 2024:012022 (6 pp.). https://doi.org/10.1088/1757-899X/1310/1/012022
DORA PSI

Jamili AM, Jhabvala J, Van Petegem S, Weisz-Patrault D, Boillat E, Nohava J, et al.
Avoiding cracks in multi-material printing by combining laser powder bed fusion with metallic foils: application to Ti6Al4V-AlSi12 structures
Additive Manufacturing. 2025; 97: 104615 (18 pp.). https://doi.org/10.1016/j.addma.2024.104615
DORA PSI

Esmaeilzadeh R, Pandiyan V, Van Petegem S, Van der Meer M, Nasab MH, de Formanoir C, et al.
Acoustic emission signature of martensitic transformation in laser powder bed fusion of Ti6Al4V-Fe, supported by operando X-ray diffraction
Additive Manufacturing. 2024; 96: 104562 (18 pp.). https://doi.org/10.1016/j.addma.2024.104562
DORA PSI

Sumarli S, Malamud F, Van Petegem S, Gaudez S, Baganis A, Busi M, et al.
Operando phase mapping in multi-material laser powder bed fusion
Virtual and Physical Prototyping. 2024; 19(1): e2429132 (17 pp.). https://doi.org/10.1080/17452759.2024.2429132
DORA PSI

Olsson M, Storm R, Björn L, Lilja V, Krupnik L, Chen Y, et al.
Phase-separated polymer blends for controlled drug delivery by tuning morphology
Communications Materials. 2024; 5: 231 (8 pp.). https://doi.org/10.1038/s43246-024-00678-y
DORA PSI

Nielsen LC, Tänzer T, Rodriguez-Fernandez I, Erhart P, Liebi M
Investigating the missing-wedge problem in smallangle X-ray scattering tensor tomography across real and reciprocal space
Journal of Synchrotron Radiation. 2024; 31(Pt 5): 1327-1339. https://doi.org/10.1107/S1600577524006702
DORA PSI

Grünewald TA, Liebi M, Birkedal H
Crossing length scales: X-ray approaches to studying the structure of biological materials
IUCrJ. 2024; 11(Pt 5): 708-722. https://doi.org/10.1107/S2052252524007838
DORA PSI

Carlsen M, Appel C, Hearn W, Olsson M, Menzel A, Liebi M
X-ray tensor tomography for small-grained polycrystals with strong texture
Journal of Applied Crystallography. 2024; 57(Pt 4): 986-1000. https://doi.org/10.1107/S1600576724004588
DORA PSI

Kermanpur A, Van Petegem S, Casati N
In-situ tensile deformation of austenitic stainless steels with various grain sizes during synchrotron and neutron diffraction
Journal of Materials Science. 2024; 59(28): 13330-13344. https://doi.org/10.1007/s10853-024-09988-5
DORA PSI

Baranowski D, Cojocariu I, Schio L, Bolaños CG, Floreano L, Dreiser J, et al.
Tuning transition metal-containing molecular magnets by on-surface polymerization
Advanced Materials Interfaces. 2024; 11(20): 2400123 (9 pp.). https://doi.org/10.1002/admi.202400123
DORA PSI

Ghanbari R, Pashazadeh S, Sekar K, Nygård K, Terry A, Liebi M, et al.
Painting Taylor vortices with cellulose nanocrystals: suspension flow supercritical spectral dynamics
Physics of Fluids. 2024; 36(4): 044114 (16 pp.). https://doi.org/10.1063/5.0195130
DORA PSI

Björn L, Persson Jutemar E, Melhado Mazza R, Andreasson E, Linell F, Guizar-Sicairos M, et al.
Process-induced structures of injection-molded high-density polyethylene─Combining X-ray scattering and finite element modeling
ACS Applied Polymer Materials. 2024; 6(8): 4852-4864. https://doi.org/10.1021/acsapm.4c00581
DORA PSI

Yang J, Schlenger LM, Nasab MH, Van Petegem S, Marone F, Logé RE, et al.
Experimental quantification of inward Marangoni convection and its impact on keyhole threshold in laser powder bed fusion of stainless steel
Additive Manufacturing. 2024; 84: 104092 (11 pp.). https://doi.org/10.1016/j.addma.2024.104092
DORA PSI

Nygård K, McDonald SA, González JB, Haghighat V, Appel C, Larsson E, et al.
ForMAX – a beamline for multiscale and multimodal structural characterization of hierarchical materials
Journal of Synchrotron Radiation. 2024; 31(Pt 2): 363-377. https://doi.org/10.1107/S1600577524001048
DORA PSI

Krupnik L, Avaro J, Liebi M, Anaraki NI, Kohlbrecher J, Sologubenko A, et al.
Iron-carbohydrate complexes treating iron anaemia: understanding the nano-structure and interactions with proteins through orthogonal characterisation
Journal of Controlled Release. 2024; 368: 566-579. https://doi.org/10.1016/j.jconrel.2024.02.044
DORA PSI

Conceição ALC, Müller V, Burandt E-C, Mohme M, Nielsen LC, Liebi M, et al.
Unveiling breast cancer metastasis through an advanced X-ray imaging approach
Scientific Reports. 2024; 14(1): 1448 (9 pp.). https://doi.org/10.1038/s41598-024-51945-4
DORA PSI

Navarre C, Van Petegem S, Schlenger L, Cayron C, Hamidi-Nasab M, Esmaeilzadeh R, et al.
Monitoring of laser-induced fast recrystallization in SS-316L through synchrotron X-ray diffraction
Materials and Design. 2024; 238: 112628 (14 pp.). https://doi.org/10.1016/j.matdes.2023.112628
DORA PSI

Silva Barreto I, Pierantoni M, Nielsen LC, Hammerman M, Diaz A, Novak V, et al.
Micro- and nanostructure specific X-ray tomography reveals less matrix formation and altered collagen organization following reduced loading during Achilles tendon healing
Acta Biomaterialia. 2024; 174: 245-257. https://doi.org/10.1016/j.actbio.2023.12.015
DORA PSI

de Formanoir C, Hamidi Nasab M, Schlenger L, Van Petegem S, Masinelli G, Marone F, et al.
Healing of keyhole porosity by means of defocused laser beam remelting: Operando observation by X-ray imaging and acoustic emission-based detection
Additive Manufacturing. 2024; 79: 103880 (18 pp.). https://doi.org/10.1016/j.addma.2023.103880
DORA PSI

Hamidi Nasab M, Masinelli G, de Formanoir C, Schlenger L, Van Petegem S, Esmaeilzadeh R, et al.
Harmonizing sound and light: X-ray imaging unveils acoustic signatures of stochastic inter-regime instabilities during laser melting
Nature Communications. 2023; 14: 8008 (14 pp.). https://doi.org/10.1038/s41467-023-43371-3
DORA PSI

Esmaeilzadeh R, Hamidi-Nasab M, de Formanoir C, Schlenger L, Van Petegem S, Navarre C, et al.
In-situ selective laser heat treatment for microstructural control of additively manufactured Ti-6Al-4V
Additive Manufacturing. 2023; 78: 103882 (14 pp.). https://doi.org/10.1016/j.addma.2023.103882
DORA PSI

Nielsen LC, Erhart P, Guizar-Sicairos M, Liebi M
Small-angle scattering tensor tomography algorithm for robust reconstruction of complex textures
Acta Crystallographica Section A: Foundations and Advances. 2023; 79(6): 515-526. https://doi.org/10.1107/S205327332300863X
DORA PSI

Gao S, Li Z, Van Petegem S, Ge J, Goel S, Vas JV, et al.
Additive manufacturing of alloys with programmable microstructure and properties
Nature Communications. 2023; 14(1): 6752 (11 pp.). https://doi.org/10.1038/s41467-023-42326-y
DORA PSI

Pfeiffer S, Florio K, Makowska M, Aneziris CG, Van Swygenhoven H, Wegener K, et al.
Crack-reduced laser powder bed fused oxide ceramic parts by in-situ synthesis of negative thermal expansion phases
Journal of the European Ceramic Society. 2024; 44(2): 1012-1026. https://doi.org/10.1016/j.jeurceramsoc.2023.09.040
DORA PSI

Makowska MG, Verga F, Pfeiffer S, Marone F, Chang CST, Florio K, et al.
Operando tomographic microscopy during laser-based powder bed fusion of alumina
Communications Materials. 2023; 4: 73 (15 pp.). https://doi.org/10.1038/s43246-023-00401-3
DORA PSI

Björn L, Melhado Mazza R, Andreasson E, Linell F, Lutz-Bueno V, Guizar-Sicairos M, et al.
Scanning small-angle X-ray scattering of injection-molded polymers: anisotropic structure and mechanical properties of low-density polyethylene
ACS Applied Polymer Materials. 2023; 5(8): 6429-6440. https://doi.org/10.1021/acsapm.3c01007
DORA PSI

Tsolaki E, Corso P, Zboray R, Avaro J, Appel C, Liebi M, et al.
Multiscale multimodal characterization and simulation of structural alterations in failed bioprosthetic heart valves
Acta Biomaterialia. 2023; 169: 138-154. https://doi.org/10.1016/j.actbio.2023.07.044
DORA PSI

Olsson M, Govender R, Diaz A, Holler M, Menzel A, Abrahmsén-Alami S, et al.
Multiscale X-ray imaging and characterisation of pharmaceutical dosage forms
International Journal of Pharmaceutics. 2023; 642: 123200 (10 pp.). https://doi.org/10.1016/j.ijpharm.2023.123200
DORA PSI

Gh Ghanbari P, Markovic P, Van Petegem S, Makowska MG, Wrobel R, Mayer T, et al.
A close look at temperature profiles during laser powder bed fusion using operando X-ray diffraction and finite element simulations
Additive Manufacturing Letters. 2023; 6: 100150 (9 pp.). https://doi.org/10.1016/j.addlet.2023.100150
DORA PSI

Godard P, Verezhak M, Sadat T, Mignerot F, Jacques VLR, Le Bolloc'h D, et al.
In situ compression of micropillars under coherent X-ray diffraction: a case study of experimental and data-analysis constraints
Journal of Applied Crystallography. 2023; 56(2): 381-390. https://doi.org/10.1107/S1600576723000493
DORA PSI

Simutis G, Bollhalder A, Zolliker M, Küspert J, Wang Q, Das D, et al.
In situ uniaxial pressure cell for x-ray and neutron scattering experiments
Review of Scientific Instruments. 2023; 94: 013906 (7 pp.). https://doi.org/10.1063/5.0114892
DORA PSI

König H-H, Holländer Pettersson N, Durga A, Van Petegem S, Grolimund D, Chuang AC, et al.
Solidification modes during additive manufacturing of steel revealed by high-speed X-ray diffraction
Acta Materialia. 2023; 246: 118713 (11 pp.). https://doi.org/10.1016/j.actamat.2023.118713
DORA PSI

Lo Re G, Engel ER, Björn L, Guizar Sicairos M, Liebi M, Wahlberg J, et al.
Melt processable cellulose fibres engineered for replacing oil-based thermoplastics
Chemical Engineering Journal. 2023; 458: 141372 (8 pp.). https://doi.org/10.1016/j.cej.2023.141372
DORA PSI

Silva Barreto I, Pierantoni M, Hammerman M, Törnquist E, Le Cann S, Diaz A, et al.
Nanoscale characterization of collagen structural responses to in situ loading in rat Achilles tendons
Matrix Biology. 2023; 115: 32-47. https://doi.org/10.1016/j.matbio.2022.11.006
DORA PSI

Chen M, Simonelli M, Van Petegem S, Tse YY, Chang CST, Makowska MG, et al.
A quantitative study of thermal cycling along the build direction of Ti-6Al-4V produced by laser powder bed fusion
Materials and Design. 2023; 225: 111458 (11 pp.). https://doi.org/10.1016/j.matdes.2022.111458
DORA PSI

Härtel M, Illgen C, Panzner T, Bruder E, Schmaltz S, Van Petegem S, et al.
Mechanical, microstructural and in-situ neutron diffraction investigations of equi-biaxial Bauschinger effects in an interstitial-free DC06 steel
International Journal of Plasticity. 2022; 159: 103478 (19 pp.). https://doi.org/10.1016/j.ijplas.2022.103478
DORA PSI

Chen M, Van Petegem S, Zou Z, Simonelli M, Tse YY, Chang CST, et al.
Microstructural engineering of a dual-phase Ti-Al-V-Fe alloy via in situ alloying during laser powder bed fusion
Additive Manufacturing. 2022; 59: 103173 (10 pp.). https://doi.org/10.1016/j.addma.2022.103173
DORA PSI

Pandiyan V, Masinelli G, Claire N, Le-Quang T, Hamidi-Nasab M, de Formanoir C, et al.
Deep learning-based monitoring of laser powder bed fusion process on variable time-scales using heterogeneous sensing and operando X-ray radiography guidance
Additive Manufacturing. 2022; 58: 103007 (15 pp.). https://doi.org/10.1016/j.addma.2022.103007
DORA PSI

Pauzon C, Van Petegem S, Hryha E, Chang CST, Hocine S, Van Swygenhoven H, et al.
Effect of helium as process gas on laser powder bed fusion of Ti-6Al-4V studied with operando diffraction and radiography
European Journal of Materials. 2022; 2(1): 422-435. https://doi.org/10.1080/26889277.2022.2081622
DORA PSI

Glerum JA, Hocine S, Chang CST, Kenel C, Van Petegem S, Casati N, et al.
Operando X-ray diffraction study of thermal and phase evolution during laser powder bed fusion of Al-Sc-Zr elemental powder blends
Additive Manufacturing. 2022; 55: 102806 (12 pp.). https://doi.org/10.1016/j.addma.2022.102806
DORA PSI

Pfeiffer S, Florio K, Makowska M, Marone F, Yüzbasi S, Aneziris CG, et al.
Crack-reduced alumina/aluminum titanate composites additive manufactured by laser powder bed fusion of black TiO_2-x doped alumina granules
Journal of the European Ceramic Society. 2022; 42(8): 3515-3529. https://doi.org/10.1016/j.jeurceramsoc.2022.02.046
DORA PSI

Polatidis E, Shukla S, Čapek J, Van Petegem S, Casati N, Mishra RS
Unveiling the interplay of deformation mechanisms in a metastable high entropy alloy with tuned composition using synchrotron X-ray diffraction
Materials Today Communications. 2022; 30: 103155 (9 pp.). https://doi.org/10.1016/j.mtcomm.2022.103155
DORA PSI

Ghasemi-Tabasi H, de Formanoir C, Van Petegem S, Jhabvala J, Hocine S, Boillat E, et al.
Direct observation of crack formation mechanisms with operando laser powder bed fusion X-ray imaging
Additive Manufacturing. 2022; 51: 102619 (11 pp.). https://doi.org/10.1016/j.addma.2022.102619
DORA PSI

Ghasemi-Tabasi H, Larcher MND, Cayron C, Jhabvala J, Van Petegem S, Kalentics N, et al.
Understanding variant selection and texture in additively manufactured red-gold alloys
Scripta Materialia. 2022; 211: 114490 (7 pp.). https://doi.org/10.1016/j.scriptamat.2021.114490
DORA PSI