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Electrochemistry Laboratory (LEC)

  • About LEC
  • Scientific Highlights
  • People
  • Research Groups
    • Battery Materials and Diagnostics
    • Battery Electrodes and Cells
    • Electrocatalysis and Interfaces
    • Fuel Cell Systems and Diagnostics
      • - Fuel Cell Systems
      • - Fuel Cell Diagnostics
      • - People
      • - Publications
      • - Partners
      • - Infrastructure and Services
    • Membranes and Electrochemical Cells
    • Neutron Imaging of Electrochemical Systems
      • NRES Projects
        • Patterned Wettability GDLs
        • Evaporative Cooling
        • PEWE Water Management
      • NRES Methods
        • Full Size Imaging
        • In plane imaging
        • Multi-cell
        • Losses Breakdown
        • GDL Dark field imaging
        • Water/Ice Distinction
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    • Former Electrochemical Energy Storage
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Instruments and Tools

Test facilities

  • Fuel cell test facilities for power dissipation up to 35 kW
  • Battery test facilities for up to 300 cells
  • Water electrolysis test benches for pressure up to 20 bar and 200 A power supply
  • High-pressure water electrolysis test bench for pressure up to 100 bar
  • Redox flow test system (Scribner 857) with 7 A and 10 A potentiostat
  • Tensile testing (Materials Tester Zwick/Roell Z005 with climate chamber)

In situ/operando analytical tools

  • Electrochemical Impedance Spectroscopy for up to 80 A DC current (Biologic)
  • Gas analyzer for CO2 using NDIR with range of to 0.1 and 1 %
  • Mass Spectrometry for gas analysis
  • Differential Electrochemical Mass Spectrometry (DEMS)
  • X-ray diffraction (in-house and in collaboration with Material Science Beamline at SLS)
  • FTIR/ATR Spectrometer (Bruker Vertex 70v) with electrochemical cell
  • Combined Raman and FTIR Microscope (HORIBA Jobin Yvon) with electrochemical cells
  • Electrochemical X-ray absorption spectroscopy (in collaboration with SuperXAS / Phoenix Beamline at SLS) with electrochemical cell
  • Neutron Imaging (in collaboration with NEUTRA and ICON Beamlines at SINQ)
  • Neutron Diffraction (in collaboration with HRPT Beamline at SINQ) with electrochemical cell
  • X-Ray Tomographic Microscopy (in-house using GE Nanotom m and in collaboration with Tomcat Beamline at SLS) with electrochemical cells
  • Helox/Oxygen gain measurements with Pulsed Gas Analysis (PGA)
  • XPS Photoelectron Spectrometer (Escalab 220i XL) for solid state batteries with electrochemical cell

Standard analytical tools

  • XPS Photoelectron Spectrometer (Escalab 220i XL)
  • Scanning Electron Microscope (SEM/EDX/STEM) with Broad Ion Beam Sample Preparation
  • Small Angle X-ray Scattering/X-ray diffraction (SAXS/XRD, Rigaku)
  • TGA and DSC calorimetric analysis
  • Standard electrochemical equipment (CV, EIS, RRDE, galvanostatic charge/discharge)
  • In-plane and through-plane membrane conductivity cell (Scribner)
  • Karl Fischer Test (Water content determination)
  • Oxygen gas sensor educatec 0-27 % +/- 1% (GDX O2 sensor with Bluetooth interface)

Preparation

  • Membrane preparation facilities (area 25 x 25 cm2)
  • Infrastructure for non-aqueous electrochemistry (glove box, electrochemical cells)
  • Catalyst Synthesis facilities

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Contact

Electrochemistry Laboratory
Paul Scherrer Institut
5232 Villigen-PSI
Switzerland

Laboratory Head a.i.
Dr. Felix N. Büchi
Telephone: +41 56 310 24 11
E-mail: felix.buechi@psi.ch


Secretary
Cordelia Gloor
Telephone: +41 56 310 29 19
E-mail: cordelia.gloor@psi.ch
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