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Teaser ptychografie

Wie Katalysatoren altern

Medienmitteilungen Forschung mit Synchrotronlicht Materialforschung Zukunftstechnologien Industriezusammenarbeit

Katalysatoren, die in der Industrie eingesetzt werden, verändern über die Jahre ihre Materialstruktur. Mit einer neuen Methode haben PSI-Forschende dies nun auf der Nano-Skala untersucht.

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Dario Ferreira Sanchez

Dreidimensionaler Blick in aktive Katalysatoren

Forschung mit Synchrotronlicht Materialforschung Zukunftstechnologien

Die operando-Röntgenspektroskopie erlaubt einen Blick ins Innere laufender Chemiereaktoren. Forschende des Karlsruher Instituts für Technologie (KIT), am Paul Scherrer Institut PSI und an der European Synchrotron Radiation Facility (ESRF) in Frankreich setzen die Methode erfolgreich ein.

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Cover Materials Today

Operando X-ray diffraction during laser 3D printing

Ultra-fast operando X-ray diffraction experiments reveal the temporal evolution of low and high temperature phases and the formation of residual stresses during laser 3D printing of a Ti-6Al-4V alloy. The profound influence of the length of the laser-scanning vector  on the evolving microstructure is revealed and elucidated.  

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inside batteries

Inside Batteries

Lithium ion batteries (LIB) are essential in modern everyday life, with increasing interest in enhancing their performance and lifetime. Secondary particles of Li-rich cathode material were examined with correlated ptychographic X-ray tomography and diffraction microscopy at different stages of cycling to probe the aging mechanism.

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Figure 1 (a) Transient relative x-ray intensity of the (1.5 0.5 0.5) superlattice reflection of Sr0.97Ca0.03TiO3 upon above bandgap excitation with 40 fs pulses Inset: STO crystal structure as seen along the c-axis. phi measures the antiferrodistortive rotation of the oxygen octahedra (exaggerated) and represents the order parameter. (b) Calculated energy change per STO cubic unit cell as a function of oxygen displacement u/u0 along the in-plane cubic crystal axes resulting from the octahedral rotation at …

Moving Atoms by Photodoping

Understanding how and how fast we can drive atoms to create a structural phase transition is of fundamental interest as it directly relates to many processes in nature. Here we show that a photoexcitation can drive a purely structural phase transition before the energy is relaxed in the material that corresponds to a “warmer” equilibrated state.

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