Lab News & Scientific Highlights

Gas attenuators are important devices providing accurate variation of photon intensity for soft X-ray beamlines. In the SwissFEL ATHOS beamline front-end the space is very limited and an innovative approach has been taken to provide attenuation of three orders of magnitude up to an energy of 1200 eV. Additive manufacturing of a differential pumping system vacuum manifold allowed a triple pumping stage to be realized in a space of less than half a meter. Measurements have shown that the response of the device is as expected from theoretical calculations.

Operando X-ray diffraction was used to measure process zone temperatures in laser powder bed fusion and compared with finite element simulations.

3d transition metals often exhibit a quenched orbital moment when in a solid state system. Therefore, the proposition of a large unquenched orbital moment for V in VI₃ caused some surprise and discussion in the scientific community. Experimental and theoretical works diverge on the fact of whether the orbital moment is quenched or not. In our work we have been able to give an answer this open issue, proposing also a model for the ground state of VI₃.

The thermal conditions during laser-based additive manufacturing are inferred from high-speed X-ray diffraction data and can be linked to a model for rapid solidification.

Rare ferrimagnet states in a phase competing antiferromagnet.

High-speed in situ X-ray diffraction is used to measure temperature profiles and cooling rates during 3D printing of a a Ti-6Al-4V single-track wall.

In situ alloying is an effective method to engineer microstructures of additively manufactured Ti6Al4V3Fe alloys. 

We present a novel monitoring strategy for 3D print processes that consists of developing and training a hybrid machine learning model that can classify regimes across different time scales based on heterogeneous sensing data. 

The mechanochromism of hybrid 2D perovskites is probed at pressures compatible with practical applications

Polyoxomolybdates have been directly synthesized from basic reagents in a mechanochemical one-pot reaction.

Aerosols in the atmosphere react to incident sunlight. This light is amplified in the interior of the aerosol droplets and particles, accelerating reactions. ETH and PSI researchers have now been able to demonstrate and quantify this effect and recommend factoring it into future climate models.

The reaction of elemental scandium and zirconium powders with liquid aluminum is observed directly via operando X-ray diffraction during laser 3D printing. This work demonstrates that elemental blends can be used to create fine-grained crack-free Al-alloys and highlights the importance of feature size.

Combining time-resolved soft X-ray STXM imaging with magnetic laminography, researchers were able to investigate magnetization dynamics in a ferromagnetic microstructure resolved in all three spatial dimensions and in time. Thanks to the possibility of freely selecting the frequency of the excitation applied to the magnetic element, this technique opens the possibility to investigate resonant magneto-dynamical processes, such as e.g. magnetic vortex core gyration and switching, and spinwave emission.

PSI hosted again the Hercules School in March 2022. We had the pleasure to welcome 20 international PhD students, PostDocs and scientists to demonstrate our state-of-the-art techniques and methodologies at our large scale facilities, the Swiss Light Source (SLS), the Swiss Spallation Neutron Source (SINQ) and our free electron laser SwissFEL.

A novel approach to controlling the speed of magnetic processes has been found through resonant magnetic scattering in an antiferromagnetic Lanthanide intermetallics.

Operando high-speed X-ray radiography experiments reveal the cracking mechanism during 3D laser printing of a Ni superalloy.

Synchrotron X-ray diffraction experiments reveal the presence of a non- negligible amount of tetragonal phase in 3D printed red-gold samples. 

Scientists have used state-of-the-art 3D printing and microscopy to provide a new glimpse of what happens when taking magnets to three-dimensions on the nanoscale – 1000 times smaller than a human hair.

In an interdisciplinary project, researchers from the Laboratory of Nanoscale Biology in BIO  and the Laboratory for Condensed Matter in PSD have revealed the reaction between the nitrogen atoms of the amyloid-beta peptide and copper/zinc ions by using soft X-ray absorption spectroscopy.

This experiment performed at SwissFEL shows how fast we can localize electrons out of an electron gas into correlated, well localized states of a material. It is based on a combined ultrafast x-ray absorption and diffraction experiment on an intermetallic system.