High aspect ratio X-ray optics requires heavy absorbing materials such as gold to provide the required absorption or phase contrast in X-ray imaging. Numerous technologies exist to deposit metal layers/films and examples include sputtering, atomic layer deposition and pulsed laser deposition (not limited to). Electrochemical methods such as electroplating is widely considered as a cost-effective and practical solution for a number of the applications such as microelectronics, MEMS and jewelry. However, the challenge of coating or filling very high aspect ratio in large areas requires non-conventional methods. We developed and currently utilize a number of electrochemical techniques for various metallization steps in the fabrication of X-ray optics.