Sample Environment

ZEBRA is operated in two geometrical modes:

  • 4-circle equatorial geometry (γ = 0o)
  • tilting geometry (-14.5o< γ <15o

ZEBRA has two exchangeable detector units:

  • turnable area and pointdetector (in operation)
  • point detector with analyzer unit (available mid 2017) for low background
  • open HUBER cradle with dedicated cryostats 4.5-300K (CCR3) and 1.6-30K (JT-CCR), small furnace (300K-800K) or optical furnace (up to 1200K, controlled gas atmosphere)
  • pressure cell (20 kbar, T > 6 K)
  • photocrystallography (400-800 nm, T > 50 K,100mW/cm2)
  • no magnetic field possible
  • magnetic field: 6 and 10 Tesla vertical magnets with large out-of-plane openings, 12 Tesla vertical in MA15 (small vertical opening), and 4.5 Tesla horizontal in MA7
  • cryogenics (T > ~50 mK)
  • furnaces (<2000K)
  • optical camera for centering of samples in 4-circle geometry (Eulerian cradle) at room temperature
  • neutron camera for sample alignment in sample environments 
  • kappa goniometer for small crystals transferred from a laboratory single-crystal X-ray diffractometer (STOE Stadivari available at PSI)
  • new Eulerian cradle with xyz-motorized cryostat carrier allowing diffractometric centering of samples at any temperature